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产品名称: 15%DC-550填充柱 合成三氯氢硅中聚氯硅烷与甲基氯gui烷测定
产品型号: 15%DC-550填充柱
品牌: 1356
产品数量:
产品单价: 面议
日期: 2023-01-24

15%DC-550填充柱 合成三氯氢硅中聚氯硅烷与甲基氯gui烷测定的详细资料

合成三氯氢硅中聚氯硅烷与甲基氯gui烷测定
合成三氯氢硅中聚氯硅烷与甲基氯gui烷测定 详细信息:


聚氯硅烷和甲基氯硅烷是合成三氯氢硅中的两类重要化合物。目前对这两类化合物的研究仅限于理论方面,通过实验数据进行的研究较少。

浩瀚色谱(山东)应用技术开发有限公司采用气相色谱质谱联用技术对三氯氢硅合成中的聚氯硅烷形态进行了解析,确认六氯二硅烷是主要聚氯硅烷,其次是六氯二硅氧烷和五氯二硅烷;通过间接测试的方法实现了甲基氯硅烷与三氯氢硅、四氯化硅在DC550s色谱柱上的完全分离;并对合成氯硅烷中甲基氯硅烷的形态进行了分析和确认,其主要甲基氯硅烷有甲基二氯硅烷、二甲基氯硅烷、甲基三氯硅烷。



合成三氯氢硅中聚氯硅烷与甲基氯gui烷测定 谱图:




Determination of Polychlorosilane and Methylchlorogui in Synthetic Trichlorosilane

Details of determination of polychlorosilane and methylchlorogui in synthetic trichlorosilane:


Polychlorosilane and methylchlorosilane are two important compounds in the synthesis of trichlorosilane. At present, the research on these two kinds of compounds is limited to theoretical aspects, and the research through experimental data is less.


Haohan Chromatography (Shandong) Applied Technology Development Co., Ltd. analyzed the form of polychlorosilane in the synthesis of trichlorosilane by gas chromatography and mass spectrometry, and confirmed that hexachlorodisilane is the main polychlorosilane, followed by hexachlorodisiloxane and pentachlorodisilane; The complete separation of methylchlorosilane, trichlorosilane and tetrachlorosilane on DC550s column was achieved by indirect test; The morphology of methylchlorosilane in synthetic chlorosilane was analyzed and ///confirm/i/i/ied. The main methylchlorosilane was methyldichlorosilane, dimethylchlorosilane and methyltrichlorosilane.



Determination spectrum of polychlorosilane and methylchlorogui in synthetic trichlorosilane: