| 产品名称: |
1/4*3.5in Tenax-TA吸附管测定食品塑料包装材料中挥发性有机物 |
| 产品型号: |
1/4*3.5in |
| 品牌: |
1356 |
| 产品数量: |
|
| 产品单价: |
面议 |
| 日期: |
2022-09-29 |
1/4*3.5in Tenax-TA吸附管测定食品塑料包装材料中挥发性有机物的详细资料
Tenax-TA吸附管测定食品塑料包装材料中挥发性有机物
Tenax-TA吸附管测定食品塑料包装材料中挥发性有机物 详细信息:
名称:吸附柱/采样管
型号:Tenax-TA
粒度:60-80目
应用:室内空气,环境空气,固定污染源废气,建筑室内空气TVOC
浩瀚色谱(山东)应用技术开发有限公司采用顶空-气相色谱法测定了食品用软质塑料包装材料中具有代表的10种挥发性有机物(VOC′s),包括甲苯、乙酸乙酯、2,4-戊二酮、2-乙基-1-己醇、1-壬醛、癸烷醛、十二烷醛、癸烷、正辛烷及十二烷,并用基体匹配法抵消了样品本身的基体干扰。从待分析样品(包装膜)裁取约100cm2大小片样置于真空烘箱中,于90℃烘24h,此片试样即可作为空白基质,再加入一定量的上述VOC标准溶液制备校准曲线。另取同一样品一片,剪碎后移入顶空瓶中,立即盖紧,在100℃平衡30min。方法中用HP-INNOWAX色谱柱在20℃~220℃温度区间程序升温,对各VOC进行分离,采用火焰离子化检测器检测。测得10种VOC′s的检出限(3S/N)在0.2~2.0μg.dm-2之间。另测得平均回收率及相对标准偏差(n=6)分别在82.5%~97.6%和0.9%~14.0%之间。
Tenax-TA吸附管测定食品塑料包装材料中挥发性有机物 测试谱图:

Determination of volatile organic compounds in food plastic packaging materials by Tenax-TA adsorption tube
Determination of volatile organic compounds in food plastic packaging materials by Tenax-TA adsorption tube Details:
Name: adsorption column/sampling tube
Model: Tenax-TA
Granularity: 60-80 mesh
Application: indoor air, ambient air, statio
nary pollution source exhaust gas, building indoor air TVOC
Haohan Chromatography (Shandong) Application Technology Development Co., Ltd. used headspace-gas chromatography to determine 10 representative volatile organic compounds (VOC's) in flexible plastic packaging materials for food, including toluene, ethyl acetate, 2, 4-pentanedione, 2-ethyl-1-hexanol, 1-nonanal, decanal, dodecanal, decane, n-octane and dodecane, and the matrix matching method was used to offset the sample itself. Matrix interference. Cut out a
bout 100 cm2 of the sample to be analyzed (packaging film), put it in a vacuum oven, and bake it at 90 °C for 24 h. This sample can be used as a blank matrix, and then a certain amount of the above VOC standard solution is added to prepare a calibration curve. Take another piece of the same sample, cut it into pieces and transfer it into a headspace vial, close it immediately, and equilibrate at 100°C for 30min. In the method, the HP-INNOWAX column was used to program the temperature in the temperature range of 20℃~220℃, and the VOCs were separated and detected by flame io
nization detector. The detection limits (3S/N) of 10 kinds of VOC's are between 0.2~2.0μg.dm-2. The average recovery and relative standard deviation (n=6) were also measured between 82.5%-97.6% and 0.9%-14.0%, respectively.
Determination of volatile organic compounds in food plastic packaging materials by Tenax-TA adsorption tube Test spectrum: