产品名称：	5Å+GDX-502填充柱 二甲胺羰基化制备N,N二甲基甲酰胺的原料一氧化碳测定
产品型号：	5Å+GDX-502填充柱
品牌：	1356
产品数量：
产品单价：	面议
日期:	2022-09-25

5Å+GDX-502填充柱 二甲胺羰基化制备N,N二甲基甲酰胺的原料一氧化碳测定的详细资料

二甲胺羰基化制备N,N二甲基甲酰胺的原料一氧化碳测定
二甲胺羰基化制备N,N二甲基甲酰胺的原料一氧化碳测定 详细信息：

二甲胺羰基化制备N,N二甲基甲酰胺(DMF)的方法.该方法采用二甲胺和一氧化碳(CO)作为反应物,在催化作用下,通过CO插入的羰基化反应制备DMF.其反应条件如下:该反应在固定床反应器中进行,反应压力1.0～8.0MPa,反应温度150～250℃,二甲胺进料空速50～800h.该方法的特征是(1)该反应具有100%的原子经济性,无副产物的生成(2)以贵金属负载的金属氧化物或分子筛为催化剂,催化剂制备简单且率催化该反应,DMF的收率可达到80%以上.

<sup>名称：填充柱1
型号：GDX-502
固定相：高分子小球
粒度：60-80目
规格：5m*1/8


名称：填充柱2
型号：5Å
固定相：分子筛
粒度：60-80目
规格：1.5m*1/8


二甲胺羰基化制备N,N二甲基甲酰胺的原料一氧化碳测定 测试谱图：</sup>



Determination of carbon monoxide as raw material for the preparation of N,N dimethylformamide by carbonylation of dimethylamine
Carbon monoxide determination of raw materials for the preparation of N,N dimethylformamide by carbonylation of dimethylamine Details:

A method for the preparation of N,N dimethylformamide (DMF) by the carbonylation of dimethylamine. This method uses dimethylamine and carbon monoxide (CO) as reactants, and under the action of catalysis, the carbonylation reaction of CO insertion is used to prepare DMF. The reaction conditions are as follows: the reaction is carried out in a fixed bed reactor, the reaction pressure is 1.0-8.0 MPa, the reaction temperature is 150-250 DEG C, and the dimethylamine feed space velocity is 50-800 h1. The method is characterized by (1) the reaction It has 100% atom economy and no by-products. (2) Using noble metal supported metal oxides or molecular sieves as catalysts, the catalyst is simple to prepare and catalyzes the reaction with high efficiency, and the yield of DMF can reach more than 80%.

Name: Packed Column 1
Model: GDX-502
Stationary phase: polymer beads
Granularity: 60-80 mesh
Specifications: 5m*1/8


Name: Packed Column 2
Model: 5A
Stationary Phase: Molecular Sieve
Granularity: 60-80 mesh
Specifications: 1.5m*1/8


Determination of carbon monoxide, raw material for the preparation of N,N dimethylformamide by carbonylation of dimethylamine. Test spectrum: